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Analysis of radioactive materials:
The coulometric methods are hugely used in the determination of uranium and plutonium and therefore search extensive use in the nuclear energy field. Reduction of UO22+ to U4+ can be carried out in H2SO4 medium with a mercury pool cathode at- 0.60 V vs. SCE. Sample holding 7-75 mg of uranium might be analysed along with an accuracy of ± 0.1%.
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