Instrumentation:

Experimental setup of TT consists of a reagent delivery system (motor driven automated buret), an adiabatic reaction cell (such as Dewar flask with stirring device), an electronic temperature sensing system and an amplifying and data processing system. A typical experimental assembly and adiablatic cell are illustrated in Figures respectively. In TT temperature control is most important and depends upon the results required. Often, it is possible to obtain and paint in titrations simply by bringing both the sample and the titrant to room's temperature. However, for precise calorimetric results the titrant and sample must be close to the same temperature as far as possible and this is achieved by a thermostat.

Figure: Schematic layout for thermometric titration assembly and bridge circuit

Figure: An efficient adiabatic cell for thermometric titrations