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Assignment Help: >> Extraction of Anionic Metal Complexes - Equilibria

Equilibria:

Fe(III), Cd (II) and Zn (II) are known to be extracted by high molecular weight amines from hydrochloric acid medium. The relevant equilibria steps for extraction by a tertiary amine or a quarternary ammonium salt are given below:

Fea3+ + 4 Cl-a ↔         FeCl-4

R3No +HCla ↔ R3NH+Cl-o

R3NH+Cl-o + FeCl-4a ↔ R3NH+FeCl-4o + Cl-a

Likewise, in quaternary ammonium salt, the extraction will follow the step:

R3R´N+Cl-o   + FeCl-4 ↔ R R´N+. FeCl-4o   + Cl -a                                             

The extraction equilibria steps for Zn(II) and Cd(II) chlorocomplexes will be as follows:

 Zn2+a+4Cl-a↔ ZnCl2-4a                                                                                                            

 2 R3NH+Clo- + ZnCl 2-4a ↔ (R3NH+)2.ZnCl2-4o +2Cl-a                                    

2 R3R'N+Clo- + ZnCl 2-4a ↔ (R3R'N+)2.ZnCl2-4o +2Cl-a                                    

Cd 2+a +4Cl-a↔ CdCl2-4a                                                                                                        

 2 R3NH+Clo- + CdCl 2-4a ↔ (R3NH+)2.CdCl2-4o +2Cl-a      

 2 R3R'N+Clo- + CdCl 2-4a ↔ (RRN+)2.CdCl2-4o +2Cl-a         

Likewise, the nitrate and sulphate complexes of different metals are extracted from the corresponding mineral acids.

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