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Nebulisation techniques:
The accuracy, precision and detection limits of flame AAS depend on how the analyte sample is introduced into the atomiser. We need to transfer a reproducible and representative portion of a sample into an atomiser which depends on the physical and chemical state of the analyte and the sample matrix. The sample introduction is achieved with the help of a nebuliser. The generally used nebulisation techniques are ultrasonic nebulisation, pneumatic nebulisation, electrothermal vaporisation and hydride generation.
Atomic absorption spectrophotometry (AAS) is now a routinely and widely employed technique for trace and ultratrace analysis of complex matrices of geological, biological, glass, environmental, industrial, cement, marine sediment, pharmaceutical, engine oil or any other kind of samples. An atomic absorption techniques using flame are rapid and precise and are applicable to about 67 elements. The electrothermal methods of analysis instaed are slower and less precise; thus, these are more sensitive and require much smaller samples
H-C=CH-CH-c
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An element X with the electronic configuration 1s 2 , 2s 2 , 2p 6 , 3s 2 , would be expected to form the chloride with the formula: (1) XCl 3 (2) Xcl 2 (3) XCl
The magnetic quantum number for an electron when the value of principal quantum number is 2 can have: (1)3 values (2) values (3)9 values (4)6 values Ans: 3 values
Radioanalytical methods: Radioanalytical methods using radiotracers and activation analysis are more sensitive and specific because of ease of detection of nuclear radiation.
State the function along with one example each of: (i) Antihistamines (ii) Antioxidants (b) What are hybrid propellants?
What is the purpose of zone refining One refining process is based on the fact that the first solid to crystallize in a two component system is usually purer than the liquid as
A 15 m 3 tank contains steam at 10 bar and 300 o C. The system is then cooled until the temperature reaches 150 o C . Some of the steam condenses. a) How much heat was transf
The energy of second Bohr orbit of the hydrogen atom is -328 kJ mol-1, hence the energy of fourth Bohr orbit would be: (1) - 41 kJ mol -1 (2) -1312 kJ mol -1 (3) -164
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