Already have an account? Get multiple benefits of using own account!
Login in your account..!
Remember me
Don't have an account? Create your account in less than a minutes,
Forgot password? how can I recover my password now!
Enter right registered email to receive password!
Define Procedure for Estimation of Iron in the Solution?
Carry out the experiment following the steps enumerated herewith:
1. Weigh 702 mg of reagent grade ferrous ammonium sulphate (NH4)2Fe (SO4)2. Dissolve it in 1000 ml distilled water. Add 5 ml of conc. sulphuric acid (or 3ml of 18 M sulphuric acid). 1 ml contains 0.100 mg of ferrous iron. Warm slightly and add 5 ml concentrated potassium permanganate (KMnO4) drop by drop until it produces a permanent colour (light pink). KMnO4 is added to oxidize the ferrous to ferric. Transfer this solution to a 1 litre volumetric flask and make the volume to 1 litre mark with distilled water. This solution contains 0.1 mg iron/ml.
2. Label a series of Borosil test tubes with blank (B), standard (Sl-S6) and sample (SA 1-4) and place them in a rack.
3. Take different volumes (0.2,0.4,0.6,0.8, 1.0 and 1.2 ml) of standard solution in the labeled tubes and make the volume to 2rnl with distilled water. Add 0.5 ml conc. sulphuric acid, 1 ml potassium persulphate and 2 ml of potassium thiocyanate to all tubes. Mix. Keep for 5 minutes for colour development. Add 9.5 ml distilled water to all tubes, mix and measure the optical density at 490nm.
4. For unknown sample make up the volume upto 100 ml of the given solution. Take 0.6 ml and 0.8 ml of the solution in duplicate and proceed just as in case of standard.
5. Draw the standard curve and calculate the amount of unknown solution present.
How to Calculate the Mass of Atoms in AMU's ? To calculate the masses of atoms we need only know the numbers of the various subatomic particles within the nucleus. For our purp
Define Pollutants Regulated Under the Clean Water Act? The Federal Water Pollution Control Act (FWPCA) Amendments of 1972 later amended while the Clean Water Act (CWA) organize
Determine the hierarchical order of soil taxanomy Order: At this highest level of generalisation, the soils are distinguished on the basis of the degree of horizon developme
Evidence Favouring the Big Bang One piece of evidence comes from the expansion of the universe which we have already described. The expanding universe suggests that the matt
Comment on their location in the sky (constellation, relative altitude over the horizon, etc) and track their movement above the course of the next couple of weeks, every day comme
Food Chain: As you know from the discussion of the previous subsection, one of the ways in which the organisms are related is through food, that is, one organism becomes food
Hard and soft water in cleaning Prepare two samples of dirty cloth. Wash one in soft water with soap unless it is clean. Wash the other cloth in hard water for the similar leng
Burns : There are two types of burns which we are to discuss: 1) Chemical 2) Thermal Chemical burns have already been discussed in Sec. 16.7; so we shall discuss thermal
Few sentences about fetus in human being? Definition, development, & important notes?
Explain the Histotoxic Hypoxia It is a type of hypoxia in which due to the action of a toxic agent oxidative enzymes are poisoned hence the tissue cells cannot utilize oxygen s
Get guaranteed satisfaction & time on delivery in every assignment order you paid with us! We ensure premium quality solution document along with free turntin report!
whatsapp: +1-415-670-9521
Phone: +1-415-670-9521
Email: [email protected]
All rights reserved! Copyrights ©2019-2020 ExpertsMind IT Educational Pvt Ltd