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Every precipitate will be collected using a Hirsch funnel. Make definite that the plastic frit disc is firmly snapped in place in your focus. Replacement frit discs are available in case it become clogged or otherwise broken. Attach the funnel to a filter flask, using the neoprene adapter to ensure a good seal among the funnel and the flask. Attach the filter flask to your vacuum line and turn the vacuum on. Swirl the precipitate in solution and quickly pour the mixture onto the filter (while the solids are still suspended). Rinse the precipitate with a minimal amount of ice-cold water. Leave the space on until the precipitate is dry (~5 min.), and take note of the mass.
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Borax bead test : The transparent glassy bead while heated along with inorganic salt and the colour produced gives some idea of cation present in it. Table:
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Ring substitution in aromatic ethers Alkoxy group is ortho and para directing and it directs the incoming groups to ortho and para position. It becomes the aromatic ring leads
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