atomic absorption troublshouting, Chemistry

atomic absorption troublshouting, Chemistry

Assignment Help:

Dear sir,
We need your consultancy in a technical problem that we are confronting, and we would really appreciate your help
We are in the process of implementing the heavy metal analysis in fish and water by atomic atomic absorption spectroscopy,
I’m still in the sample preparation optimization phase, and I’m confronting some problems,

Il explain in brief the problem in my last results obtained:
For arsenic analysis, 0.2 g sample is digested with Nitric acid At 90?C for 45 min ,then placed in oven for 2 hours at 130 ?C, then diluted to desired volume

1- 0.2 g Unknown fish sample spiked with (2.5ml) 1000ppb arsenic standard, after dilution in 25 ml H2O,the theoretical value must be 100 ppb, but the practical value came out 75 ppb
2- 0.2 g Fish muscle certified reference material ,containing 12.7 mg/kg of arsenic, and since the dilution is in 50 ml, then the theoretical value must be 50.8 ppb, the practical value came out 0.57ppb

Knowing that both samples were treated in the same condition and in the same time, the difference in the end results is very weird, please advise concerning any note that can improve our work,
or detect any mistake has been made,
waiting for your reply,many thanks in advance

Related Discussions:- atomic absorption troublshouting

Factors that affects crystallization of organic compound, What are the 5 Fa...

What are the 5 Factors that affects crystallization of organic compounds?

Conversion of caco3 equivalent, Q. A sample of water analysis was found t...

Q. A sample of water analysis was found to contain temporary magnesium hardness 25 mg/L. Permanent magnesium chloride hardness 15 mg/L and permanent calcium sulphate hardness 20

Explain two characteristic superstructures, If lipids are mixed with water,...

If lipids are mixed with water, what aggregates can they form? Explain two characteristic superstructures which are commonly found in biological systems, containing our food. How i

POLYMERS, SHORTNOTE ON CONDUCTING POLYMERS

SHORTNOTE ON CONDUCTING POLYMERS

Disaccharides - biomolecules, Disaccharides - Biomolecules The disacch...

Disaccharides - Biomolecules The disaccharides give in on hydrolysis two monosaccharides. Those disaccharides that generates two hexoses on hydrolysis contain a general formul

#title metallocarborans, defination and examples

defination and examples

Normality, equation ..

equation ..

Organic chemistry, perkin ring clousre reaction

perkin ring clousre reaction

Need of tar, If you have not used tar before, try this sequence to makeanar...

If you have not used tar before, try this sequence to makeanarchive ofyour llast project: %cd;tar cf llast.tar llast %tar tfv llast.tar The first line m vesyou to your hom

Chemical equation, Li + H20 ----> LiOH + H2....if I start with 3.4 mols of ...

Li + H20 ----> LiOH + H2....if I start with 3.4 mols of H2O , how many mols of H2 can I make?

Write Your Message!

Name

Email id

Message

Verfication Code

Free Assignment Quote

Assured A++ Grade

Get guaranteed satisfaction & time on delivery in every assignment order you paid with us! We ensure premium quality solution document along with free turntin report!

Submit Assignment

All rights reserved! Copyrights ©2019-2020 ExpertsMind IT Educational Pvt Ltd