State the synthesis of aspirin from methyl salicylate

Reference no: EM13181429

Durning the synthesis of Aspirin from Methyl salicylate we perfom a recrystallization. How do I relate the % yield of each compound to the efficacy of the recrystallization technique?

The instructions are listed below:

Rinse the crystals several times with small portions (2 mL) of ice-cold water and air dry the crystals on a Buchner funnel by suction until the crystals appear to be free of solvent. Record the weight of the crude solid which probably contains water.

To recrystallize: Dissolve the final product in a minimum amount (no more than 1 mL) of hot ethanol in a 25 mL Erlenmeyer flask. Make sure that the product is completely dissolved while gently and continuously heating on a steam bath.

Pour 5 ml of hot water into the flask, then let the flask cool at room temperature for 10 minutes and cool in an ice bath for an additional 5 minutes. Collect the product by vacuum filtration and rinse out of the flask with a few milliliters of cold water.

Reference no: EM13181429

Questions Cloud

State nitrogen gas in container : The second container is kept at 149.2 K. What is the volume (in liters) of nitrogen gas in container 2? Containers are kept at a constant pressure.

State the synthesis of phenyl magnesium bromide : Based on your observations, what might have happened if you had not followed these instructions? Might this also have affected your percent yield? Explain.

Explain the partial pressure of o2 : A mixture of N2 and O2 gases are in a 2.0L container at 23 degrees C and at a total pressure of 1.00 atm.

Describes a thioester and reduced cofactor : Determine whether each of the phrases or examples describes a thioester, reduced cofactor, or phosphorylated compound:

State the synthesis of aspirin from methyl salicylate : Durning the synthesis of Aspirin from Methyl salicylate we perfom a recrystallization. How do I relate the % yield of each compound to the efficacy of the recrystallization technique?

Describe maximization of income : If the price of blue toy cars is $5 and the price of pink toy cars is $2, then which of the following consumers will make the same choices if their income is the same (assuming maximization of income) Gloria, utility is U(b,p) = b^2 * p

Balanced equation for the synthesis of acetylsalic acid : What is the balanced equation for the synthesis of Acetylsalic acid (Aspirin) from Methyl salicylate?

Determine the cost to the government of buying firms : Consider a market where supply and demand are given Qx^s=-10 +Px and Qx^d= 56-2Px. Suppose the government imposes a price floor of $25, and agrees to purchase any and all units concumers do not buy at the floor price of $235 per unit. a. Determine..

How many configurations of occupied : Probability question. A doctor's office has 4 examination rooms. At any given time, each room can either be occupied or empty. How many configurations of occupied and empty examination rooms are possible?

User Account

All Pages