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Methyl-1-hexanol (A) was reacted with NaBr/H2SO4 to give (B), which upon treatment with magnesium in diethyl ether formed an intermediate (C) which was not isolated. Reaction of (C) with dry ice gave, after the appropriate work-up (D).
a) write the equation which describe the above sequence, including structures for compounds (A) to (D)
b) If the yield in the conversion of (A) to (B) was 65% and that of (B) to (D), via (C) was 75% , what is the overall yield of (D) to (A)?
c)Assuming the above yields, how much of (A), in grams, is required in order to produce 0.75 mol of (D)?
2) Why is anhydrous ether used in this reaction?3) Why is the water bath used to heat the reaction?4) What is the mechanism of the reaction of phenylmagnesium bromide and CO2? Include the workup steps.5) In this experiment, it is important to use freshly obtained dry ice. Why?
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The flask was then shaken until the solution was uniform. A 40.0-mL sample of this glucose solution was diluted to 0.500 L. How many grams of glucose are in 100 mL. of the final solution?
Thomas used equimolar amounts of diethylamine and alpha chloro-2,6-dimethylacetanilide in the preparation of Lidocaine. All the starting material reacted but failed to isolate any Lidocaine.
The heat of solution of ammonium chloride (NH4Cl(s)) in water is +14.7 kJ/mol. Calculate the mass (in g) of NH4Cl(s) required to change the temperature of (1.2550x10^2) ml of water from (2.440x10^1) °C to (5.30x10^0) °C.
A sample of gas in a balloon has an initial temperature of 3degrees celsius and a volume of 1740 L. If the temperature changes to 88 degrees celsius , and there is no change of pressure or amount of gas, what is the new volume, V2, of the gas
what weight of A would be removed from a solution of 10g of A in 100mL of water by a single extraction of 100mL lingroin. what weight of A would be removed by four successive extractions with 25mL portions of lingroin
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