Reference no: EM133148050
Question 1) Provide an experimental description of what you did. (As you would find in the supporting information of a journal article). This should include NMR data and a yield. Please see the help sheet provided on Learning Central.
Question 2) Draw a curly arrow mechanism for this reaction 140o
Question 3) Copy your TLC here with labels: include the description of each spot, the solvent system and the Rf value for each spot, mark on where the solvent front is. You could attach a photo instead if you prefer but still annotate.
Question 4) Annotate the H-NMR spectrum of 1-(4-bromophenyl)-5-methyl-3-fluoromethyl-1H-pyrazole) given below. The Annotation includes a drawing of the compound and assignment of the peaks.
Question 5) Affix your 1H NMR spectrum to this page and compare it to the one has been given above indicating which peaks are the same. Justify any missing or extra peaks. Confirm if you had the formation of the expected compound.
Question 6) Annotate the C-NMR spectrum of 1-(4-bromophenyl)-5-methyl-3-fluoromethyl-1H-pyrazole) given below. The Annotation includes a drawing of the compound and assignment of the peaks
Question 7) Affix your 13C NMR spectrum to this page and compare it to the one has been given above indicating which peaks are the same. Justify any missing or extra peaks. Confirm if you had formation of the desired compound.