Construct a vector grid of the pair-wise subtraction

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(a) Construct a 4x4 vector grid of the pair-wise subtraction of the equivalent positions of the space group. Summarize the vector peaks in this grid w.r.t. uvw type, vector peaks (in terms of x, y, z) and multiplicity.

(b) Use the information above to determine the fractional coordinates of a chlorine atom. Confirm the position with that of a general uvw peak.

(c) From (b) determine the positions of the other 3 chlorine atoms.

(d) Explain which Patterson peak probably does not represent a Cl···Cl vector?

(e) Use the chlorine position in (b) to calculate F(311) using the structure factor equation below for a centrosymmetric structure. Explicitly state what the phase angle is in radians.

Reference no: EM132711700

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