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Exp: The reduction of 4-t-Butylcyclohexanone using Sodium borohydride(NaBH4).
1. Suggest another separation method that might be used to determine the cis to trans ratio of products from this reaction.
* Gas Chromatography (GC) has been used to estimate the relative Yield of cis and trans isomer.
2. Clearly label the axial and equatorial substituents on each of the two products of this reaction in their most stable conformation (ignore the hydrogen atoms).
3. When a small base (e.g. NaBH4) is used in the experiment, the trans product is favoured, but when a bulky based is used, the cis product is favoured. Both reactions are irreversible. Provide an explanation for the selectivity of each base.
Show all the steps in the mechanism for the following reaction, When benzene is mixed with deuterated sulfuric acid, deuterium is slowly incorporated onto the ring. Show the mechanism for this reaction and explain how this relates the sulfonation of ..
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